manuais Metrohm 757 VA Computrace

Metrohm 757 VA Computrace Manual do Utilizador (198 páginas)

Marca: Metrohm | Categoria: Software | Tamanho: 3.45 MB |

Alemão

Índice

757 VA Computrace

1

Inhaltsverzeichnis

3

Betriebsart «Exploratory»

5

Betriebsart «Determination»

6

Fehlerbehebung

9

Softwarelizenzvereinbarung

10

1 Einführung

11

1.2 Allgemeine Informationen

12

1.3 Installation

13

1.6 Kontext-sensitive Menüs

20

2 Hauptfenster

21

2.3 Menü «File»

24

2.4 Menü «Mode»

26

2.5 Menü «Utility»

27

2.6 Menü «User»

27

2.7 Menü «Settings»

31

2.8 Menü «Window»

35

3 Allgemeine Einstellungen

37

«Determination»

37

Voltage step time

38

Drop size

38

[ 1...9 ; 4 ]

38

Stirrer/RDE (rpm)

40

[ 0...3000 rpm ; 2000 rpm ]

40

3.2 VA-Messmodi

41

DC - Sampled direct current

45

EXPLORATORY SPECIFICATION

45

WORKING METHOD

45

SPECIFICATIONS

45

NP - Normal pulse

47

Potential limit (V)

52

[ -5...+5 V ; -0.1 V ]

52

Maximum time (s)

52

[ > 0 ; 20 s ]

52

3.3 Potentiostat

55

3.5 Grafische Einstellungen

59

Width [ 0...8 ; 0 ]

64

4 Betriebsart «Exploratory»

65

4.2 Fenster

66

Exploratory specification

66

4.3 Signalkurven

70

Exploratory

80

5.2 Arbeitsmethode

82

5.3 Monitor

98

<Next>

99

757 VA Computrace – Software

100

5.4 Bestimmungskurven

104

DETERMINATION CURVES

105

5.5 Resultate

113

5.6 Probentabelle

118

Determination

121

Determination method

122

Working method

122

Order [ 1...6 ; ]

122

Sample table

122

BASELINE

126

Front end

126

Rear end

126

Peak voltage

127

Peak height

127

Derivative

127

Peak area

127

CALCULATION

130

No. of replications

132

DETERMINATION

133

6 Handbedienung

135

6.2 Dosimat-Steuerung

137

6.3 Filmbildung

138

6.4 Reinigung

140

6 Handbedienung

142

7 Wie gehe ich vor ...?

143

7.2 Anwenderzugriffsrechte

144

7.5 Bestimmungen

151

7.7 Kalibrierkurven-Technik

160

7.9 Diagnose

166

8 Fehlerbehebung

171

8.3 Softwareprobleme

172

8.4 Dosimatprobleme

172

8.6 Voltammetrische Probleme

177

Deposition time

181

Deposition potential

181

Polynomial

187

Exponential

187

8 Fehlerbehebung

190

Index

193

Metrohm 757 VA Computrace Manual do Utilizador (82 páginas)

Marca: Metrohm | Categoria: Software | Tamanho: 2.36 MB |

Inglês

Índice

757 VA Computrace

1

Table of contents

3

List of figures

4

1 Introduction

5

1.2.1 Organization

6

1.3 Support documentation

8

1.3 Support documentation

9

1.3.2 Application Notes

10

1.3.3 Monographs

10

1.3.4 Reprints

10

2 Parts and controls

11

3 Installation

17

3.2.3 Connection to the PC

19

3.2.5 Inert gas connection

23

757 VA Computrace – Hardware

25

MAIN WINDOW /

29

Utility / Computrace control

29

COMPUTRACE CONTROL

29

PUTRACE CONTROL

30

3.3.6 Storing the MME

34

3.3.9 Cleaning the MME

36

3.4.2 Regenerating the RDE

38

3.5 Reference electrode

40

3.5.2 Startup procedure

41

3.6 Auxiliary electrode

42

3.7 Stirrer

43

3.8.2 Tubing connection

45

3.9.1 Electrical connection

47

6.2141.150 Cable

48

6.2141.080 Cable

48

3.9.2 Tubing connections

50

3.9.3 Software settings

52

4 Safety

55

4.2.1 Properties of mercury

56

4.2.3 Handling of mercury

57

4 Safety

60

5 Technical data

61

6 Appendix

65

6.2 Options

72

6.3 Warranty

75

EU Declaration of Conformity

76

6.6 Index

78

6.6 Index

79

6 Appendix

80

Metrohm 757 VA Computrace Manual do Utilizador (198 páginas)

Marca: Metrohm | Categoria: Software | Tamanho: 3.42 MB |

Inglês

Índice

757 VA Computrace

1

Table of contents

3

Exploratory mode

5

Determination mode

6

Troubleshooting

9

Software license

10

1 Introduction

11

1.2 General information

12

1.3 Installation

13

Method 2

16

1.5 Overview of file types

20

1.6 Context sensitive menus

20

2 Main window

21

2.3 File menu

24

2.4 Mode menu

26

2.5 Utility menu

27

2.6 User menu

27

2.7 Settings menu

31

2.8 Window menu

35

3 General settings for

37

Voltage step

38

Drop size

38

[ 1...9 ; 4 ]

38

Stirrer/RDE (rpm)

40

[ 0...3000 rpm ; 2000 rpm ]

40

3.2 VA measurement modes

41

SqW - Square wave

43

EXPLORATORY SPECIFICATION

43

WORKING

43

METHOD SPECIFICATIONS

43

DC - Sampled direct current

45

WORKING METHOD SPECIFICATIONS

45

NP - Normal pulse

47

CV - Cyclic voltammetry

49

Potential limit (V)

52

[ -5...+5 V ; -0.1 V ]

52

Maximum time (s)

52

[ > 0 ; 20 s ]

52

3.3 Potentiostat

55

3.5 Graphical settings

59

Width [ 0...8 ; 0 ]

64

4 Exploratory mode

65

4.3 Exploratory curves

70

5 Determination mode

81

Voltammetric

87

WORKING METHOD SPECIFI

87

5.3 Monitor

98

<Next>

99

757 VA Computrace – Software

100

5.4 Determination curves

104

DETERMINATION CURVES

105

TERMINATION CURVES

105

5.5 Results

113

Substance

115

Substances

115

Cell volume

115

5.6 Sample table

118

Determination method

122

Working method

122

Order [ 1...6 ; ]

122

Sample table

122

BASELINE

126

Front end

126

Rear end

126

Peak voltage

127

Peak height

127

Derivative

127

Peak area

127

CALCULATION

130

No. of replications

132

6 Manual control

135

6.2 Dosimat control

137

6.3 Film deposition

138

6.4 Cleaning procedure

140

6 Manual control

142

7 How to ...?

143

7.2 User rights

144

Measure blank

150

No. of blanks

150

Blank purge time

150

<OK>

150

7.5 Determinations

151

7.9 Diagnostic procedures

166

END OF DETERMINA

170

8 Troubleshooting

171

8.3 Software problems

172

8.4 Dosimat problems

172

8.6 Voltammetric problems

177

Deposition time

181

Deposition potential

181

Exponential

187

8 Troubleshooting

190

Index

193

Metrohm 757 VA Computrace Manual do Utilizador (81 páginas)

Marca: Metrohm | Categoria: Software | Tamanho: 2.30 MB |

Alemão

Índice

757 VA Computrace

1

Inhaltsverzeichnis

2

Verzeichnis der Abbildungen

3

1 Einleitung

4

1.2.1 Aufbau

5

1.3.1 Applikations-Bulletins

7

1.3.2 Application Notes

9

1.3.3 Monographien

9

1.3.4 Nachdrucke

9

2 Bedienungs

10

Details siehe

14

3 Installation

16

3.2.3 Anschluss am PC

18

3.2.5 Inertgas-Anschluss

22

757 VA Computrace – Hardware

24

3.3.3 Kapillare montieren

27

757 VA COMPUTRA

28

COMPUTRACE

28

CONTROL

28

COMPUTRACE CONTROL

29

3.3.6 Aufbewahren der MME

33

3.3.8 Wechsel der Kapillare

34

MME herausziehen

35

3.4.2 Regenerierung der RDE

37

3.5 Bezugselektrode

39

3.5.2 Inbetriebnahme

40

3.6 Hilfselektrode

41

3.7 Rührer

42

3.8.1 Elektrischer Anschluss

43

3.8.2 Schlauchanschluss

44

3.9.1 Elektrischer Anschluss

46

Kabel 6.2141.150

47

Kabel 6.2141.080

47

3.9.2 Schlauchverbindungen

49

3.9.3 Softwareeinstellungen

51

4 Sicherheit

54

4 Sicherheit

59

5 Technische Daten

60

Elektrodentips 6.1204.XXX

61

Material

62

6 Anhang

64

6.2 Optionen

71

6.3 Gewährleistung

74

6.4 EU-Konformitätserklärung

75

EU Konformitätserklärung

75

Systemvalidierung

76

6.6 Index

77

6.6 Index

78

6 Anhang

79

Metrohm 757 VA Computrace Manual do Utilizador (198 páginas)

Marca: Metrohm | Categoria: Software | Tamanho: 2.29 MB |

Francês

Índice

757 VA Computrace

1

Table des matières

3

757 VA Computrace – Software

10

1 Introduction

11

1.2 Informations générales

12

1.3 Installation

13

2 Fenêtre principale

21

2.3 Menu «File»

24

2.4 Menu «Mode»

26

2.5 Menu «Utility»

27

2.6 Menu «User»

27

2.7 Menu «Settings»

31

2.8 Menu «Window»

35

3 Réglages généraux pour

37

Drop size [ 1...9 ; 4 ]

39

Surface

40

3.2 Modes de mesure VA

41

Sampled direct current

45

Mode dans la fenêtre

45

SPECIFICATIONS

45

NP - Normal pulse

47

SPECIFICATION

47

METHOD SPECIFICATIONS

49

3.3 Potentiostat

55

3.5 Réglages graphiques

59

Width [ 0...8 ; 0 ]

64

0 = Ligne fine)

64

4 Mode d'utilisation

65

«Exploratory»

65

4.3 Courbes de signaux

70

5 Mode d'utilisation

81

5.2 Méthode de travail

82

5.3 Monitor

98

<Next>

99

MONITOR

99

DETERMINATION CURVES

105

5.5 Résultats

113

«Determination»

121

Determination method

122

Working method

122

Order [ 1...6 ; ]

122

Sample table

122

Front end ou Rear end

126

Peak voltage

127

Peak height

127

Derivative

127

Peak area

127

RESULTS

130

CALCULATION

130

DETERMINATION

133

6 Maniement

135

6.2 Commande de Dosimate

137

6.3 Formation de film

138

6.4 Procédure de nettoyage

140

6 Maniement

142

7 Comment procéder...?

143

7.5 Déterminations

151

7.9 Diagnostic

166

<OK>

170

END OF DETERMINATION

170

8 Traitement des erreurs

171

8.3 Problèmes de logiciel

172

End potential du sweep

177

Voltage step

178

METHOD PARAMETERS

178

Deposition potential

181

Contrat de concession de

191

Index

193

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