Metrohm 887 Professional UV/VIS Detector Manual do Utilizador

887 Professional UV/VIS Detector2.887.0010Manual8.887.8003EN

1.3 About the documentation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector1.3 About the documentationCautionPlease read through this

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭3WarningThis symbol draws attention to a possible biologicalhazard.Caution

1.4 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4￭￭￭￭￭￭￭￭887 Professional UV/VIS DetectorMains voltageWarningAn incorrect mains voltage can damage the in

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭51.4.5 Recycling and disposalThis product is covered by European Directiv

2.1 Front￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector2 Overview of the instrument2.1 Front12Figure 1 Front1Detector block2Standby

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭71Mains switchFor switching the instrument on and off.I = On

3.1 Setting up the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector3 Installation3.1 Setting up the instrument3.1.1 Packag

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭92.887.00102.886.01102.850.xxxx2.872.xxxx2.850.xxxx2.872.xxxx2.887.00102.8

3.3 Mounting base tray and bottle holder (optional)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector3.3 Mounting base tray and bottle

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭11Removing the base tray Before you can remove the base tray, the followin

3.3 Mounting base tray and bottle holder (optional)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭12￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector132 1Attach the base tray so that t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭1312 3 1Remove the two covering stoppers. 2Loosen the two cylinder screws

3.3 Mounting base tray and bottle holder (optional)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭14￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector12 3 1Attach the bottle holder onto

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭153.4 Capillary connections in the IC systemThis chapter contains general

3.4 Capillary connections in the IC system￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭16￭￭￭￭￭￭￭￭887 Professional UV/VIS DetectorConnection capillariesPEEK capillaries and P

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭17 2Plug the capillary all the way into the connection or coupling untilth

3.5 Installing the flow-through cell￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭18￭￭￭￭￭￭￭￭887 Professional UV/VIS DetectorInstalling the flow-through cell1234 1Loosen knurl

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭193.6 Connecting the flow-through cellTo connect the capillaries to the f

3.7 Connecting the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭20￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector3412Figure 7 Connecting detector output1Detector inlet ca

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭21￭ 6.2122.040 with plug CEE(7), VII (Germany, …)￭ 6.2122.070 with plug NE

Metrohm AGCH-9100 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 [email protected] Professional UV/VIS Detector2.887.001

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭22￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector4 Start-upThe 887 Professional UV/VIS Detector is set up together wit other instru-me

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Start-up887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭23Figure 8 Intensity spectrum okIf the intensity spectrum is cut off like the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭24￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector5 OperationThe instrument is operated via MagIC Net™ software only. Additionalinforma

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Handling and maintenance887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭256 Handling and maintenance6.1 General notes6.1.1 CareWarn

6.2 Door￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭26￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector6.1.4 Shutting downIf the instrument is not used for a longer period, the who

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Handling and maintenance887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭276.3 Replacing the UV lampAfter a certain burning time, the

6.3 Replacing the UV lamp￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭28￭￭￭￭￭￭￭￭887 Professional UV/VIS DetectorRemoving old UV lampWarningAfter longer operation, the UV lam

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Handling and maintenance887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭291234Figure 12 Lamp module – without UV lamp1Lamp cooling ele

6.4 Replacing the VIS Lamp￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭30￭￭￭￭￭￭￭￭887 Professional UV/VIS DetectorAlign the groove on the lamp socket with the bolt in the ope

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Handling and maintenance887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭31￭ The flow-through cell is rinsed with ultrapure water.￭ The

TeachwareMetrohm AGCH-9100 [email protected] documentation is protected by copyright. All rights reserved.Although all the information

6.6 Cleaning the flow-through cell￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭32￭￭￭￭￭￭￭￭887 Professional UV/VIS DetectorRinsing the flow-through cell with methanol 1Disconn

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Handling and maintenance887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭33If the noise persists, the flow-through cell must be dismant

6.6 Cleaning the flow-through cell￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭34￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector1Retaining screw2Outer seal3Lens4Inner seal5Measurin

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Handling and maintenance887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭356.7 Quality Management and validation with MetrohmQuality M

7.1 Problems and their solutions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭36￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector7 Troubleshooting7.1 Problems and their solutionsPro

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Technical specifications887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭378 Technical specifications8.1 Reference conditionsThe tech

8.3 Lamps￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭38￭￭￭￭￭￭￭￭887 Professional UV/VIS DetectorAnalog outputVoltage range–1.0…+1.0 VResolution30 µVNoise< 30 µVOutput imp

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Technical specifications887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭398.4 Ambient conditionsOperationAmbient tem-perature+5…+45 °

8.6 Mains connection￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭40￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector8.6 Mains connectionRequired voltage100…240 V (±10%)Required fre-

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Conformity and warranty887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭419 Conformity and warranty9.1 Declaration of ConformityThis

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭IIITable of contents1 Introduction 11.1 Instrument description ...

9.2 Quality Management Principles￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭42￭￭￭￭￭￭￭￭887 Professional UV/VIS DetectorMetrohm Ltd. is holder of the SQS certificate ISO 900

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Conformity and warranty887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭43ManufactureThe measures put into practice in the production o

10.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭44￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector10 AccessoriesNoteSubject to change without notice.10.1 Scope o

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10 Accessories887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭45Qty. Order no. Description1 6.2151.020 Cable USB A - USB B / 1.8 mUSB co

10.2 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭46￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector10.2 Optional accessories 2.887.0010 887 Professional UV/VI

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10 Accessories887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭47Order no. Description6.2804.100 Halogen lamp (VIS) for UV/VIS instrument

10.2 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭48￭￭￭￭￭￭￭￭887 Professional UV/VIS DetectorOrder no. Descriptionlanguages: German, English, French, Span

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Index887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭49IndexAAccessoriesOptional ... 46Ambient conditions ...

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭IV￭￭￭￭￭￭￭￭887 Professional UV/VIS Detector6 Handling and maintenance 256.1 General notes ...

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of figures887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭VTable of figuresFigure 1 Front ...

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction887 Professional UV/VIS Detector￭￭￭￭￭￭￭￭11 Introduction1.1 Instrument descriptionThe 887 Professional UV/VIS Det