Metrohm 792 Basic IC Manual do Utilizador Página 34
- Página / 197
- Índice
- MARCADORES
Avaliado. / 5. Com base em avaliações de clientes
2.6 High-pressure pump
792 Basic IC
25
2.6.3 Connecting the eluent bottle
To connect the eluent bottle with the high-pressure pump, insert the
supplied 6.1834.010 aspirating tubing (i.d. = 1.5 mm, e.d. = 2.5 mm,
length = 2.5 m) into one of the openings
5
55
5
or
7
77
7
in the interior of the 792
Basic IC. Pull the aspirating tubing sufficiently far into the interior of the
792 Basic IC and push at least 5 mm of it onto aspirating capillary
32
3232
32
(see
Fig. 3
) of the high-pressure pump (it may be necessary to use em-
ery paper). Screw on the 6.2821.090 aspirating filter at the other end of
the aspirating tubing and insert it into the eluent bottle.
Only degassed (with N
2
, He or vacuum) and microfiltered (0.45
P
m
filter) eluents should be used!
Care must be taken that the eluent used is freely miscible with any
solvent remaining in the pump head (the pump head leaves the
factory filled with either isopropanol or methanol/water). If this is not
the case then the pump must first be rinsed with a solvent which is
miscible with both the previous eluent and the following eluent (e.g.
acetone).
2.6.4 Deaerating the pump and rinsing the pulsation dampener
The first time that it is started up the high-pressure pump must be
deaerated. Proceed as follows:
1 Prepare for deaeration
x
Open the rotary knob on purge valve
31
3131
31
by approx. ½ turn in
the counterclockwise direction (see
Fig. 3
).
x
Mount a PEEK compression fitting
46
4646
46
(see
section 2.3.4
) to
the end of capillary
30
3030
30
and screw coupling
24
2424
24
(6.2744.120) to
the compression fitting
46
4646
46
.
x
Push 6.2816.020 Syringe (without needle) into the connection
on coupling
24
2424
24
until the stop is reached.
2 Open system
x
Start the
«
792 Basic IC
»
PC program, if it has not been al-
ready been started (see
section 2.5.3
).
x
Select
File / Open / System
in the main window and open the
folder
Default
. Select the system file
Default.smt
and click on
<Open>
. The corresponding system window is opened:
- BasicBasic 1
- Table of contents 2
- Notes – Maintenance – Faults 5
- Appendix 6
- List of figures 7
- 1 Introduction 10
- 1 Introduction 15
- 1.733.0110 Detector block) 15
- 1.3.1 Organization 17
- SYSTEM STATE 18
- <OK> 18
- 1.4 Safety notes 19
- 2 Installation 20
- 2.2.1 Packaging 22
- 2.2.2 Check 22
- 2.2.3 Location 22
- 2.3.5 Filter unit PEEK 25
- 2.4 Mains connection 26
- 2.4.2 Fuses 27
- 2.5 Connection to the PC 28
- 2.5.3 Basic settings 29
- Hardware 31
- Hardware settings 31
- Cell constant 31
- 2.6 High-pressure pump 32
- File / Open / System 34
- Default.smt 34
- <Open> 34
- 2 mL/min 35
- <Send to unit> 35
- Injector 38
- Flow rate 39
- <On> 39
- <Off> 39
- 2.8 Suppressor module 44
- 2.9 Putting into operation 50
- Suppressed anion 51
- Prep MSM.smt 51
- Startup determination 52
- 2 Installation 53
- 3 Operating tutorial 54
- 3.2 Preparations 55
- 3.3 Calibration 56
- <Concentrations> 61
- <Calibrate> 61
- 3.4 Sample determination 63
- 4 Operation 66
- 4.1.2 Glossary 67
- 4.1.4 Main window elements 69
- 4.1.9 Help 72
- 4.2.1 Fonts 73
- 4.2.2 Security system 73
- 4.2.3 Global settings 74
- 4.2.4 COM port 76
- 4.3 Systems 77
- 4.3.3 System functions 78
- 4.3.4 PC icon 80
- 4.3.5 Watch window 80
- 4.3.6 Instrument icon 81
- 4.3.7 System state window 87
- 4.3 Systems 88
- Error messages 88
- 4.4 Methods 89
- Data Log 95
- <Add new> 95
- New comment 95
- 4.4.3 Method setup 96
- 4.4.4 Integration 99
- 792 Basic IC 100
- 792 Basic IC 101
- Component table 103
- Components table 105
- 4.4.6 Report output 115
- 4.5 Chromatograms 127
- 4.5.4 Peak editor 136
- 4.5.5 Printing 138
- 4.6 Batch reprocessing 141
- REPROCESS / 145
- <Merge> 145
- Appearance 145
- File / Save / Chroma 145
- 5.1.1 Separating columns 148
- 5.1.2 High-pressure pump 149
- 5.1.3 Eluents 150
- 5.1.4 Peristaltic pump 150
- 5.1.5 Suppressor module 151
- 5.1.6 Connections 151
- 5.2.1 General information 152
- 5.2.2 Passivation 152
- 5.2.3 Recycling 153
- 5.2.4 Shutdown 153
- 90 and 158
- 5.3 Faults and malfunctions 165
- 6 Appendix 168
- 6.1.3 Injection valve 169
- 6.1.4 High-pressure pump 169
- 6.1.5 Peristaltic pump 170
- 6.1.6 Suppressor module 170
- 6.1.7 RS232 interface 170
- 6.1.8 Mains connection 171
- 6.1.9 Safety specifications 171
- 6.1.11 Ambient temperature 172
- 6.1.12 Housing 172
- 6.2 Standard equipment 173
- 6.3 Optional accessories 176
- 6.3 Optional accessories 178
- 6 Appendix 179
- 6.4 Warranty and conformity 185
- EU Declaration of Conformity 186
- 6.5 Index 188
- 6.5 Index 190
Manuais e produtos relacionados com Equipamento Metrohm 792 Basic IC
(27 páginas)
(156 páginas)
Equipamento Metrohm 792 Basic IC Manual do Utilizador
(197 páginas)
(197 páginas)
Equipamento Metrohm 761 Compact IC Manual do Utilizador
(229 páginas)
(229 páginas)
© 2020, manymanuals-pt.com. Todos os direitos reservados. | 0.052 s |
Manymanuals.com
Manymanuals.de
Manymanuals.fr
Manymanuals.it
Manymanuals.pl
Manymanuals.cz
Manymanuals.es
Manymanuals-pt.com
Comentários a estes Manuais